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https://doi.org/10.1007/BF02546878
Title: | A thermal analysis evaluation of the low temperature synthesis of BaBiO3 | Authors: | Chuah, G.K. Jaenicke, S. Chan, K.S. Khor, S.T. Hill, J.O. |
Keywords: | BaBiO3 EGA IR low temperature synthesis metal-organic precursors TG XRD |
Issue Date: | Oct-1993 | Citation: | Chuah, G.K., Jaenicke, S., Chan, K.S., Khor, S.T., Hill, J.O. (1993-10). A thermal analysis evaluation of the low temperature synthesis of BaBiO3. Journal of Thermal Analysis 40 (3) : 1157-1164. ScholarBank@NUS Repository. https://doi.org/10.1007/BF02546878 | Abstract: | Thermal decomposition of metal-organic precursors for the mixed oxide BaBiO3 was studied using TG and EGA. Precursors produced by polyesterification of bifunctional acids with ethylene glycol (Pechini process) decomposed about 100°C higher than those without the diol. BaCO3 was identified by IR and XRD as a reaction intermediate. EGA proved that the amount of BaCO3 was below 10% of the total barium, and that the barium exists mainly as a nitro-compound up to 650°C. Phase-pure BaBiO3 with a moderately high surface area (1.4 m2/g) could be synthesised from a citrate precursor by the Pechini process at around 850°C. © 1993 John Wiley & Sons, Limited and Akadémiai Kiadó. | Source Title: | Journal of Thermal Analysis | URI: | http://scholarbank.nus.edu.sg/handle/10635/93022 | ISSN: | 03684466 | DOI: | 10.1007/BF02546878 |
Appears in Collections: | Staff Publications |
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