Please use this identifier to cite or link to this item: https://doi.org/10.1007/BF02546878
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dc.titleA thermal analysis evaluation of the low temperature synthesis of BaBiO3
dc.contributor.authorChuah, G.K.
dc.contributor.authorJaenicke, S.
dc.contributor.authorChan, K.S.
dc.contributor.authorKhor, S.T.
dc.contributor.authorHill, J.O.
dc.date.accessioned2014-10-16T08:19:30Z
dc.date.available2014-10-16T08:19:30Z
dc.date.issued1993-10
dc.identifier.citationChuah, G.K., Jaenicke, S., Chan, K.S., Khor, S.T., Hill, J.O. (1993-10). A thermal analysis evaluation of the low temperature synthesis of BaBiO3. Journal of Thermal Analysis 40 (3) : 1157-1164. ScholarBank@NUS Repository. https://doi.org/10.1007/BF02546878
dc.identifier.issn03684466
dc.identifier.urihttp://scholarbank.nus.edu.sg/handle/10635/93022
dc.description.abstractThermal decomposition of metal-organic precursors for the mixed oxide BaBiO3 was studied using TG and EGA. Precursors produced by polyesterification of bifunctional acids with ethylene glycol (Pechini process) decomposed about 100°C higher than those without the diol. BaCO3 was identified by IR and XRD as a reaction intermediate. EGA proved that the amount of BaCO3 was below 10% of the total barium, and that the barium exists mainly as a nitro-compound up to 650°C. Phase-pure BaBiO3 with a moderately high surface area (1.4 m2/g) could be synthesised from a citrate precursor by the Pechini process at around 850°C. © 1993 John Wiley & Sons, Limited and Akadémiai Kiadó.
dc.description.urihttp://libproxy1.nus.edu.sg/login?url=http://dx.doi.org/10.1007/BF02546878
dc.sourceScopus
dc.subjectBaBiO3
dc.subjectEGA
dc.subjectIR
dc.subjectlow temperature synthesis
dc.subjectmetal-organic precursors
dc.subjectTG
dc.subjectXRD
dc.typeArticle
dc.contributor.departmentCHEMISTRY
dc.description.doi10.1007/BF02546878
dc.description.sourcetitleJournal of Thermal Analysis
dc.description.volume40
dc.description.issue3
dc.description.page1157-1164
dc.identifier.isiutA1993LZ49100034
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