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|Title:||A thermal analysis evaluation of the low temperature synthesis of BaBiO3|
|Authors:||Chuah, G.K. |
low temperature synthesis
|Citation:||Chuah, G.K., Jaenicke, S., Chan, K.S., Khor, S.T., Hill, J.O. (1993-10). A thermal analysis evaluation of the low temperature synthesis of BaBiO3. Journal of Thermal Analysis 40 (3) : 1157-1164. ScholarBank@NUS Repository. https://doi.org/10.1007/BF02546878|
|Abstract:||Thermal decomposition of metal-organic precursors for the mixed oxide BaBiO3 was studied using TG and EGA. Precursors produced by polyesterification of bifunctional acids with ethylene glycol (Pechini process) decomposed about 100°C higher than those without the diol. BaCO3 was identified by IR and XRD as a reaction intermediate. EGA proved that the amount of BaCO3 was below 10% of the total barium, and that the barium exists mainly as a nitro-compound up to 650°C. Phase-pure BaBiO3 with a moderately high surface area (1.4 m2/g) could be synthesised from a citrate precursor by the Pechini process at around 850°C. © 1993 John Wiley & Sons, Limited and Akadémiai Kiadó.|
|Source Title:||Journal of Thermal Analysis|
|Appears in Collections:||Staff Publications|
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