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https://doi.org/10.1002/1522-7189(199911/12)7:6<361::AID-NT79>3.0.CO;2-1
| Title: | Detection of diarrhetic shellfish poisoning toxins from tropical shellfish using liquid chromatography-selected reaction monitoring mass spectrometry | Authors: | Holmes, M.J. Teo, S.L.M. Khoo, H.W. |
Keywords: | Diarrhetic shellfish poisoning Mass spectrometry Mussels Okadaic acid Singapore |
Issue Date: | 1999 | Citation: | Holmes, M.J., Teo, S.L.M., Khoo, H.W. (1999). Detection of diarrhetic shellfish poisoning toxins from tropical shellfish using liquid chromatography-selected reaction monitoring mass spectrometry. Natural Toxins 7 (6) : 361-364. ScholarBank@NUS Repository. https://doi.org/10.1002/1522-7189(199911/12)7:6<361::AID-NT79>3.0.CO;2-1 | Abstract: | A negative mode liquid chromatography-selected reaction monitoring mass spectrometry (LC-SRM MS) method was developed to detect low concentrations of the diarrhetic shellfish poisoning (DSP) toxins okadaic acid and dinophysistoxin-1 (DTX-1). Detection relies upon monitoring the transition of negative precursor ions [M - H]- to a common fragment ion of m/z 255. Our limit of detection for okadaic acid with this method is 0.5 pg on column. LC-SRM MS has allowed us to detect persistent low concentrations of DSP toxins from Singapore shellfish. Copyright © 1999 John Wiley & Sons, Ltd. | Source Title: | Natural Toxins | URI: | http://scholarbank.nus.edu.sg/handle/10635/111722 | ISSN: | 10569014 | DOI: | 10.1002/1522-7189(199911/12)7:6<361::AID-NT79>3.0.CO;2-1 |
| Appears in Collections: | Staff Publications |
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