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https://doi.org/10.1016/S0022-3697(99)00010-4
Title: | Thermal stability of mesoporous silica molecular sieve | Authors: | Gu, G. Ong, P.P. Chu, C. |
Issue Date: | Jul-1999 | Citation: | Gu, G., Ong, P.P., Chu, C. (1999-07). Thermal stability of mesoporous silica molecular sieve. Journal of Physics and Chemistry of Solids 60 (7) : 943-947. ScholarBank@NUS Repository. https://doi.org/10.1016/S0022-3697(99)00010-4 | Abstract: | Mesoporous silica molecular sieves (MCM-41) with pore diameters from 3 to 10 nm were synthesized by a liquid-crystal template mechanism. A surface phonon mode at around 961 cm-1, connected with the mesoporous structure was observed. At the annealing temperature of 800 °C, the mesoporous structure of the molecular sieve was found to collapse completely, based on Fourier transform infrared spectroscopy (FTIR) and X-ray diffraction (XRD) measurements. Further annealing of MCM-41 results in transformation to the cristobalite phase of silica. | Source Title: | Journal of Physics and Chemistry of Solids | URI: | http://scholarbank.nus.edu.sg/handle/10635/98368 | ISSN: | 00223697 | DOI: | 10.1016/S0022-3697(99)00010-4 |
Appears in Collections: | Staff Publications |
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