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https://doi.org/10.1016/j.matlet.2004.09.047
Title: | The low-temperature synthesis of BiFeO 3-SrBi 2Nb 2O 9 complexes by sol-gel process | Authors: | Gu, H. Zheng, K. Chen, K. Cao, W. Wang, J. |
Keywords: | 0.1BiFeO 3-0.9SrBi 2Nb 2O 9 Nanocrystalline Sol-gel |
Issue Date: | Apr-2005 | Citation: | Gu, H., Zheng, K., Chen, K., Cao, W., Wang, J. (2005-04). The low-temperature synthesis of BiFeO 3-SrBi 2Nb 2O 9 complexes by sol-gel process. Materials Letters 59 (8-9) : 912-915. ScholarBank@NUS Repository. https://doi.org/10.1016/j.matlet.2004.09.047 | Abstract: | Nanocrystalline 0.1BiFeO 3-0.9SrBi 2Nb 2O 9 powder was successfully synthesized by a ethanolamine-modified sol-gel technique from compounds, Bi(NO 3) 3•5H 2O, Sr(NO 3) 2, Fe(NO 3) 3•9H 2O and Nb(OC 2H 5) 5 in solution ethylene glycol monomethyl ether. The powder exhibited amorphous in structure below annealing temperature 400 °C and a pure phase of layered perovskite ferroelectric structure at annealing temperature 600 °C. There was a considerable degree of particle coalescence when the xerogel was heated at 400 °C. The grains exhibited spherical shape distribution, and the average particle size of powder was in the range 50-100 nm after annealing at 700 °C. The ceramics exhibited a dense fracture surface consisting of lamellar grains. © 2004 Elsevier B.V. All rights reserved. | Source Title: | Materials Letters | URI: | http://scholarbank.nus.edu.sg/handle/10635/107238 | ISSN: | 0167577X | DOI: | 10.1016/j.matlet.2004.09.047 |
Appears in Collections: | Staff Publications |
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