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|Title:||Formation of antimony sulfide powders and thin films from single-source antimony precursors||Authors:||Castro, J.R.
|Issue Date:||2008||Citation:||Castro, J.R., Molloy, K.C., Liu, Y., Lai, C.S., Dong, Z., White, T.J., Tiekink, E.R.T. (2008). Formation of antimony sulfide powders and thin films from single-source antimony precursors. Journal of Materials Chemistry 18 (44) : 5399-5405. ScholarBank@NUS Repository. https://doi.org/10.1039/b810947h||Abstract:||Solvothermal and hydrothermal methods have been employed to generate nano-sized Sb2S3 (stibnites) from a variety of xanthate, dithiocarbamate and dithiophosphate precursors. The solvothermal method allows control of morphology by regulating precursor and size by reaction time; this process also produces near-uniform and larger particles. The xanthate precursors are far superior to the dithiocarbamates in their ability to produce oxide-free Sb2S3. Aerosol-assisted chemical vapour deposition (AACVD) provided a means to produce good quality films of Sb2S 3. The advantages of xanthate precursors is rationalised in terms of a facile, low-temperature Chugaev rearrangement. © 2008 The Royal Society of Chemistry.||Source Title:||Journal of Materials Chemistry||URI:||http://scholarbank.nus.edu.sg/handle/10635/105962||ISSN:||09599428||DOI:||10.1039/b810947h|
|Appears in Collections:||Staff Publications|
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