Please use this identifier to cite or link to this item: https://doi.org/10.1002/1521-3749(200213)628:133.0.CO;2-R
Title: Synthesis, characterization, and crystal structures of Cu, Ag, and Pd dinitramide salts
Authors: Ang, H.-G. 
Fraenk, W.
Karaghiosoff, K.
Klapötke, T.M.
Mayer, P.
Nöth, H.
Sprott, J.
Warchhold, M.
Keywords: Copper dinitramide
Crystal structure
NMR spectroscopy (multinuclear)
Palladium dinitramide
Silver dinitramide
Vibrational spectroscopy
Issue Date: 2002
Citation: Ang, H.-G.,Fraenk, W.,Karaghiosoff, K.,Klapötke, T.M.,Mayer, P.,Nöth, H.,Sprott, J.,Warchhold, M. (2002). Synthesis, characterization, and crystal structures of Cu, Ag, and Pd dinitramide salts. Zeitschrift fur Anorganische und Allgemeine Chemie 628 (13) : 2894-2900. ScholarBank@NUS Repository. https://doi.org/10.1002/1521-3749(200213)628:133.0.CO;2-R
Abstract: The literature known, but not fully characterized, silver dinitramide transfer reagents AgN(NO2)2 (1), [Ag(NCCH3)][N(NO2)2] (2), and [Ag(py)2][N(NO2)2] (3) have been investigated by 109Ag, 14N NMR and vibrational spectroscopy (IR, Raman). In addition, the poorly understood [Cu(NH3)4][N(NO2)2)]2 (4) and [Pd(NH3)4][N(NO2)2]2, (5) have also been prepared and characterized by 14N NMR and vibrational spectroscopy (IR, Raman). The structures of 2-5 have also been determined by X-ray diffraction.
Source Title: Zeitschrift fur Anorganische und Allgemeine Chemie
URI: http://scholarbank.nus.edu.sg/handle/10635/95147
ISSN: 00442313
DOI: 10.1002/1521-3749(200213)628:133.0.CO;2-R
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