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|Title:||Solid-phase synthesis of pyrazolines and isoxazolines with sodium benzenesulfinate as a traceless linker|
|Citation:||Chen, Yu., Lam, Y., Lai, Y.-H. (2003-04-03). Solid-phase synthesis of pyrazolines and isoxazolines with sodium benzenesulfinate as a traceless linker. Organic Letters 5 (7) : 1067-1069. ScholarBank@NUS Repository. https://doi.org/10.1021/ol0340888|
|Abstract:||(Matrix presented) The preparation of pyrazoline and isoxazoline derivatives with traceless solid-phase sulfone linker strategy is described. Key steps involved in the solid-phase synthetic procedure include (i) sulfinate S-alkylation, (ii) sulfone anion alkylation, (iii) γ-hydroxy sulfone → γ-ketosulfone oxidation, and (iv) traceless product release via elimination-cyclization. A library of 12 pyrazolines and isoxazolines was synthesized.|
|Source Title:||Organic Letters|
|Appears in Collections:||Staff Publications|
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