Please use this identifier to cite or link to this item: https://doi.org/10.1016/j.electacta.2004.08.048
Title: Electropolymerization of 4-nitro-1,2-phenylenediamine and electrochemical studies of poly(4-nitro-1,2-phenylenediamine) films
Authors: Yu, B.
Khoo, S.B. 
Keywords: 4-Nitro-1,2-phenylenediamine
Anodic electropolymerization
Nitro-group reduction
Poly(4-nitro-1,2-phenylenediamine) film
Polymer-modified electrodes
Issue Date: 1-Mar-2005
Citation: Yu, B., Khoo, S.B. (2005-03-01). Electropolymerization of 4-nitro-1,2-phenylenediamine and electrochemical studies of poly(4-nitro-1,2-phenylenediamine) films. Electrochimica Acta 50 (9) : 1917-1924. ScholarBank@NUS Repository. https://doi.org/10.1016/j.electacta.2004.08.048
Abstract: In this work, we report the anodic electropolymerization of 4-nitro-1,2-phenylenediamine (4NoPD) in different supporting electrolytes at different pH. The feasibilities of forming the polymer poly(4-nitro-1,2- phenylenediamine) (P4NoPD) on gold and glassy carbon electrodes (GCE) were shown. The P4NoPD films were generated by continuous potential cycling between -0.15 V and +1.10 V (versus Ag|AgCl, saturated KCl). The pH of the electropolymerization medium, the nature of the background electrolyte and the number of cycles used were found to influence strongly the amount of polymer deposited. The reduction of nitro-groups of the P4NoPD films was also found to be dependent on solution conditions, especially pH. © 2004 Elsevier Ltd. All rights reserved.
Source Title: Electrochimica Acta
URI: http://scholarbank.nus.edu.sg/handle/10635/76085
ISSN: 00134686
DOI: 10.1016/j.electacta.2004.08.048
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