Please use this identifier to cite or link to this item:
|Title:||Preparation and application of mixed octadecylsilyl- and (3-(C-methylcalixresorcinarene)-hydroxypropoxy)-propylsilyl-appended silica particles as stationary phase for high-performance liquid chromatography|
high-performance liquid chromatography
|Source:||Tan, H.M., Wang, X., Soh, S.F., Tan, S., Zhao, J., Yong, E.L., Lee, H.K., Gong, Y. (2012-03-01). Preparation and application of mixed octadecylsilyl- and (3-(C-methylcalixresorcinarene)-hydroxypropoxy)-propylsilyl-appended silica particles as stationary phase for high-performance liquid chromatography. Instrumentation Science and Technology 40 (2-3) : 100-111. ScholarBank@NUS Repository. https://doi.org/10.1080/10739149.2011.651674|
|Abstract:||A new type of mixed octadecylsily (ODS)- and (3-(C-methylcalix resorcinarene)-2-hydroxypropoxy)-propylsilyl-appended silica particles (ODS-MCR-HPS) have been prepared and used as stationary phase for high-performance liquid chromatography (HPLC) for the first time. Elemental analysis and Fourier-transform infrared spectroscopy have been applied to characterize the synthetic ODS-MCR-HPS. The new stationary phase contains two types of interaction sites for separation: ODS and MCR. The chromatographic performance of ODS-MCR-HPS was investigated by separating several disubstituted benzenes and some aromatic hydocarbons under both reversed-phase and normal-phase conditions. The results show that ODS-MCR-HPS exhibits excellent selectivity for the separation of positional isomers of disubstituted benzenes and mixtures of some aromatic hydrocarbon compounds due to the cooperative and complementary functioning of the ODS and MCR under different mobile phase conditions. Copyright © Taylor & Francis Group, LLC.|
|Source Title:||Instrumentation Science and Technology|
|Appears in Collections:||Staff Publications|
Show full item record
Files in This Item:
There are no files associated with this item.
checked on Dec 13, 2017
WEB OF SCIENCETM
checked on Nov 14, 2017
checked on Dec 16, 2017
Items in DSpace are protected by copyright, with all rights reserved, unless otherwise indicated.