Please use this identifier to cite or link to this item: https://doi.org/10.1016/S0040-4039(00)01896-7
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dc.titleSolid-phase combinatorial synthesis of benzothiazole and 2,3-dihydro-[1,5]-benzothiazepine derivatives
dc.contributor.authorLee, C.L.
dc.contributor.authorLam, Y.
dc.contributor.authorLee, S.-Y.
dc.date.accessioned2014-10-16T08:40:36Z
dc.date.available2014-10-16T08:40:36Z
dc.date.issued2001-01-01
dc.identifier.citationLee, C.L., Lam, Y., Lee, S.-Y. (2001-01-01). Solid-phase combinatorial synthesis of benzothiazole and 2,3-dihydro-[1,5]-benzothiazepine derivatives. Tetrahedron Letters 42 (1) : 109-111. ScholarBank@NUS Repository. https://doi.org/10.1016/S0040-4039(00)01896-7
dc.identifier.issn00404039
dc.identifier.urihttp://scholarbank.nus.edu.sg/handle/10635/94832
dc.description.abstractBis-(2-nitro-4-carboxyphenyl) disulfide was loaded on Wang resin and Rink amide resin. The nitro group was reduced to its amine with concomitant cleavage of the disulfide bond using SnCl2-2H2O to afford 2. Condensation of an aldehyde and nucleophilic attack on an α,β-unsaturated ketone, followed by TFA cleavage from the resin, gave benzothiazole 3 and 2,3-dihydro-[1,5]-benzothiazepine 4, respectively. © 2000 Elsevier Science Ltd.
dc.description.urihttp://libproxy1.nus.edu.sg/login?url=http://dx.doi.org/10.1016/S0040-4039(00)01896-7
dc.sourceScopus
dc.subject2,3-dihydro-[1,5]-benzothiazepine
dc.subjectBenzothiazole
dc.subjectSolid-phase synthesis
dc.typeArticle
dc.contributor.departmentCHEMISTRY
dc.description.doi10.1016/S0040-4039(00)01896-7
dc.description.sourcetitleTetrahedron Letters
dc.description.volume42
dc.description.issue1
dc.description.page109-111
dc.description.codenTELEA
dc.identifier.isiut000166025000028
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