Please use this identifier to cite or link to this item: https://doi.org/10.1016/j.chroma.2006.08.018
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dc.titleSingle laboratory validation of a method for the determination of Bisphenol A, Bisphenol A diglycidyl ether and its derivatives in canned foods by reversed-phase liquid chromatography
dc.contributor.authorSun, C.
dc.contributor.authorLeong, L.P.
dc.contributor.authorBarlow, P.J.
dc.contributor.authorChan, S.H.
dc.contributor.authorBloodworth, B.C.
dc.date.accessioned2014-10-16T08:40:24Z
dc.date.available2014-10-16T08:40:24Z
dc.date.issued2006-09-29
dc.identifier.citationSun, C., Leong, L.P., Barlow, P.J., Chan, S.H., Bloodworth, B.C. (2006-09-29). Single laboratory validation of a method for the determination of Bisphenol A, Bisphenol A diglycidyl ether and its derivatives in canned foods by reversed-phase liquid chromatography. Journal of Chromatography A 1129 (1) : 145-148. ScholarBank@NUS Repository. https://doi.org/10.1016/j.chroma.2006.08.018
dc.identifier.issn00219673
dc.identifier.urihttp://scholarbank.nus.edu.sg/handle/10635/94815
dc.description.abstractA method was developed and validated for the simultaneous determination of Bisphenol A (BPA), Bisphenol A diglycidyl ether (BADGE), BADGE-H2O, BADGE-2H2O, BADGE-H2O-HCl, BADGE-HCl, and BADGE-2HCl in canned food using reversed phase high-performance liquid chromatography (HPLC) with fluorescence detection; chromatographic separation of all seven analytes was achieved (Rs ≥ 1.08) using HPLC gradient elution technique. Acetonitrile was used to extract the analytes from the food matrix before subjecting the samples to liquid-liquid extraction, solid-phase extraction for further clean-up and preconcentration prior to HPLC analysis. Excellent inter-day precision data (n = 10) and intra-day precision data (n = 5) were obtained on a 200 μg/kg spiked sample. The RSD ranged from 0.20% to 2.96% for the inter-day precision tests, and 0.04% to 2.82% for the intra-day precision tests. Accuracy was measured at three concentration levels: 200, 1000, and 2000 μg/kg; recoveries ranged from 86.07% to 114.06%. The excellent validation data suggests that this method can be applied on canned foods for the determination of migration of BPA, BADGE and its derivatives from can coatings into food. © 2006 Elsevier B.V. All rights reserved.
dc.description.urihttp://libproxy1.nus.edu.sg/login?url=http://dx.doi.org/10.1016/j.chroma.2006.08.018
dc.sourceScopus
dc.subjectBisphenol A (BPA)
dc.subjectBisphenol A diglycidyl ether (BADGE)
dc.subjectCan coatings
dc.subjectHigh-performance liquid chromatography (HPLC)
dc.subjectMigration
dc.typeArticle
dc.contributor.departmentCHEMISTRY
dc.description.doi10.1016/j.chroma.2006.08.018
dc.description.sourcetitleJournal of Chromatography A
dc.description.volume1129
dc.description.issue1
dc.description.page145-148
dc.description.codenJCRAE
dc.identifier.isiut000240787600022
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