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Title: HPLC studies of Os3(CO)12-n(CH3CN)n (n = 0, 1, 2)
Authors: Ang, H.G. 
Kwik, W.L. 
Leong, W.K. 
Issue Date: 26-Dec-1989
Citation: Ang, H.G.,Kwik, W.L.,Leong, W.K. (1989-12-26). HPLC studies of Os3(CO)12-n(CH3CN)n (n = 0, 1, 2). Journal of Organometallic Chemistry 379 (3) : 325-330. ScholarBank@NUS Repository.
Abstract: Normal and reverse phase chromatographic separation of Os3(CO)12, Os3(CO)11- (CH3CN) and Os3(CO)10(CH3CN)2 have been examined. On a silica column good separation of these clusters can be achieved with CH2Cl2/petroleum ether as the mobile phase but better reproducibility is attained with a Hypersil ODS C18 column and a mobile phase of MeOH/CH3CN. The relative retention times correlate qualitatively with molecular structures. The identities and purities of the chromatographic peaks were determined by use of a Data Evaluation Pack. © 1989.
Source Title: Journal of Organometallic Chemistry
ISSN: 0022328X
Appears in Collections:Staff Publications

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