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|Title:||HPLC studies of Os3(CO)12-n(CH3CN)n (n = 0, 1, 2)||Authors:||Ang, H.G.
|Issue Date:||26-Dec-1989||Citation:||Ang, H.G.,Kwik, W.L.,Leong, W.K. (1989-12-26). HPLC studies of Os3(CO)12-n(CH3CN)n (n = 0, 1, 2). Journal of Organometallic Chemistry 379 (3) : 325-330. ScholarBank@NUS Repository.||Abstract:||Normal and reverse phase chromatographic separation of Os3(CO)12, Os3(CO)11- (CH3CN) and Os3(CO)10(CH3CN)2 have been examined. On a silica column good separation of these clusters can be achieved with CH2Cl2/petroleum ether as the mobile phase but better reproducibility is attained with a Hypersil ODS C18 column and a mobile phase of MeOH/CH3CN. The relative retention times correlate qualitatively with molecular structures. The identities and purities of the chromatographic peaks were determined by use of a Data Evaluation Pack. © 1989.||Source Title:||Journal of Organometallic Chemistry||URI:||http://scholarbank.nus.edu.sg/handle/10635/93972||ISSN:||0022328X|
|Appears in Collections:||Staff Publications|
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