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Title: DADD-assisted hydrothermal synthesis of t-ZrO 2 nanoparticles
Authors: Chen, F. 
Hong, Q. 
Xu, G.-Q. 
Andy Hor, T.S. 
Shen, S. 
Issue Date: Sep-2005
Citation: Chen, F., Hong, Q., Xu, G.-Q., Andy Hor, T.S., Shen, S. (2005-09). DADD-assisted hydrothermal synthesis of t-ZrO 2 nanoparticles. Journal of the American Ceramic Society 88 (9) : 2649-2651. ScholarBank@NUS Repository.
Abstract: Tetragonal ZrO 2 (t-ZrO 2) nanoparticles (diameter: ca. 10 nm; BET-specific surface area: 100 m 2/g) are hydrothermally prepared via crystallization of 1,12-diaminododecane (DADD)-hydrous zirconia gels at 230°C for 3 days. The volume content of monoelinic phase is ca. 0.1. The surface-adsorbed hydrocarbon layer (ca. 3 wt%) is observed by FTIR and TGA. They account for the formation of our t-ZrO 2 nanoparticles with high-phase purity. © 2005 The American Ceramic Society.
Source Title: Journal of the American Ceramic Society
ISSN: 00027820
DOI: 10.1111/j.1551-2916.2005.00487.x
Appears in Collections:Staff Publications

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