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|Title:||Synthesis and tuning of ordering and crystallinity of mesoporous titanium dioxide film||Authors:||Agarwala, S.
|Issue Date:||31-Jul-2009||Citation:||Agarwala, S., Ho, G.W. (2009-07-31). Synthesis and tuning of ordering and crystallinity of mesoporous titanium dioxide film. Materials Letters 63 (18-19) : 1624-1627. ScholarBank@NUS Repository. https://doi.org/10.1016/j.matlet.2009.04.036||Abstract:||Synthesis of well-organized and highly crystalline mesoporous titania (TiO2) film is demonstrated using triblock copolymer (Pluronic P123) as a structure directing template, through the evaporation induced self-assembly (EISA) process. The issue of thermal and structural stability of a mesoporous TiO2 film was addressed via optimization of annealing temperature and time. An anatase phase, high crystallinity TiO2 film with ordered pores was obtained at 430 °C after annealing for 15 min. The synthesized film was crack free with TiO2 nanoparticle size of 10-15 nm, quasi-hexagonal pore diameter in the range of 8-10 nm and film thickness of ~ 150 nm. © 2009 Elsevier B.V. All rights reserved.||Source Title:||Materials Letters||URI:||http://scholarbank.nus.edu.sg/handle/10635/83136||ISSN:||0167577X||DOI:||10.1016/j.matlet.2009.04.036|
|Appears in Collections:||Staff Publications|
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