Please use this identifier to cite or link to this item: https://doi.org/10.1166/jnn.2007.684
Title: Controlling the synthetic pathways of TiO 2-derived nanostructured materials
Authors: Lim, S.H.
Ji, W. 
Lin, J. 
Keywords: Hydrothermal
Layered titanate
Nanotubes
Nanowires
Post-synthesis treatment
Issue Date: Sep-2007
Citation: Lim, S.H., Ji, W., Lin, J. (2007-09). Controlling the synthetic pathways of TiO 2-derived nanostructured materials. Journal of Nanoscience and Nanotechnology 7 (9) : 3294-3300. ScholarBank@NUS Repository. https://doi.org/10.1166/jnn.2007.684
Abstract: A comprehensive study of the hydrothermal synthesis of TiO 2-derived nanostructured materials, including layered protonic trititanate (H 2Ti 3O 7), metal-ion exchangeable titanate (Na xH 2-xTi 3O 7), TiO 2(B) and anatase nanotubes and TiO 2-anatase nanowires, was conducted. Nanoscaled tubular structures were found to be already present in the samples derived from prolonged hydrothermal process of bulk anatase TiO 2 and could be converted to various types of nanotubes, nanowires or nanorodes by post-synthesis treatments. 0.1 M HCl acid wash and air annealing were the two key parameters to select the types of nanotubes/nanowires as the final products. XRD, Raman, TG, and XPS core level and valence band studies were carried out to elucidate our proposed synthetic pathways. Copyright © 2007 American Scientific Publishers All rights reserved.
Source Title: Journal of Nanoscience and Nanotechnology
URI: http://scholarbank.nus.edu.sg/handle/10635/96102
ISSN: 15334880
DOI: 10.1166/jnn.2007.684
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