Please use this identifier to cite or link to this item: https://doi.org/10.1016/j.chroma.2004.01.050
Title: Development and application of polymer-coated hollow fiber membrane microextraction to the determination of organochlorine pesticides in water
Authors: Basheer, C. 
Suresh, V. 
Renu, R.
Lee, H.K. 
Keywords: Extraction methods
Hollow fiber membrane
Organochlorine compounds
Pesticides
Water analysis
Issue Date: 16-Apr-2004
Citation: Basheer, C., Suresh, V., Renu, R., Lee, H.K. (2004-04-16). Development and application of polymer-coated hollow fiber membrane microextraction to the determination of organochlorine pesticides in water. Journal of Chromatography A 1033 (2) : 213-220. ScholarBank@NUS Repository. https://doi.org/10.1016/j.chroma.2004.01.050
Abstract: A novel extraction procedure coupled with gas chromatography-mass spectrometric detection for quantification of organochlorine pesticides (OCPs) in water is described. Amphiphilic polyhydroxylated polyparaphenylene (PH-PPP) was synthesized and coated on the surfaces of a porous polypropylene hollow fiber membrane (HFM). Due to the high porosity of the HFM, maximum active surface area to achieve high extraction efficiency is expected. The polymer-coated HFM was used for the extraction of 15 OCPs from water. The extraction efficiency was compared with emerging and established methods such as liquid-phase microextraction (LPME), solid-phase microextraction (SPME) and stir bar sorptive extraction (SBSE) techniques. We term the current procedure as polymer-coated hollow fiber microextraction (PC-HFME). PC-HFME showed good selectivity and sensitivity. Detection limits for OCPs were in the range of 0.001-0.008μgl-1. The sensitivity and selectivity of the coated HFM could be adjusted by changing the characteristics of the coated PH-PPP film. © 2004 Elsevier B.V. All rights reserved.
Source Title: Journal of Chromatography A
URI: http://scholarbank.nus.edu.sg/handle/10635/93569
ISSN: 00219673
DOI: 10.1016/j.chroma.2004.01.050
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