Please use this identifier to cite or link to this item: https://doi.org/10.4028/www.scientific.net/AMR.415-417.715
Title: The nanocrystallinity enhancement of sol-gel derived TiO 2 nanoparticles by pre-hydrothermal treatment
Authors: Yuwono, A.H.
Zhang, Y. 
Wang, J. 
Keywords: Enhanced nanocrystallinity
Nanocomposites
Pre-hydrothermal treatment
TiO 2
Issue Date: 2012
Citation: Yuwono, A.H., Zhang, Y., Wang, J. (2012). The nanocrystallinity enhancement of sol-gel derived TiO 2 nanoparticles by pre-hydrothermal treatment. Advanced Materials Research 415-417 : 715-719. ScholarBank@NUS Repository. https://doi.org/10.4028/www.scientific.net/AMR.415-417.715
Abstract: Nanocomposite thin film containing TiO 2 nanoparticles in polymethyl methacrylate (PMMA) is a new class of potential materials for optoelectronic applications. Among the various processing techniques for these nanocomposites, in situ sol-gel process is well known to be versatile as it enables control of the inorganic-organic interaction at various molecular, nanometer and micrometer scales. However, the resulting TiO 2 phase is largely amorphous, as a consequence of the relatively low processing temperatures. Therefore, the current research is aimed at enhancing the nanocrystallinity of TiO 2 nanoparticles in nanocomposites. For this purpose, pre-hydrothermal treatment was carried on the inorganic sols. The nanocrystallinity degree of the resulting TiO 2 nanoparticles was studied by XRD and FTIR. The studies showed that the nanocrystallinity of TiO 2 nanoparticles synthesized from the inorganic sol can be enhanced significantly by the pre-hydrothermal treatment, as a result of the completion of hydrolysis stage during sol-gel process.
Source Title: Advanced Materials Research
URI: http://scholarbank.nus.edu.sg/handle/10635/86967
ISBN: 9783037853252
ISSN: 10226680
DOI: 10.4028/www.scientific.net/AMR.415-417.715
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