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https://doi.org/10.1016/j.matlet.2009.04.036
Title: | Synthesis and tuning of ordering and crystallinity of mesoporous titanium dioxide film | Authors: | Agarwala, S. Ho, G.W. |
Keywords: | Anatase Mesoporous Sol-gel Titanium dioxide |
Issue Date: | 31-Jul-2009 | Citation: | Agarwala, S., Ho, G.W. (2009-07-31). Synthesis and tuning of ordering and crystallinity of mesoporous titanium dioxide film. Materials Letters 63 (18-19) : 1624-1627. ScholarBank@NUS Repository. https://doi.org/10.1016/j.matlet.2009.04.036 | Abstract: | Synthesis of well-organized and highly crystalline mesoporous titania (TiO2) film is demonstrated using triblock copolymer (Pluronic P123) as a structure directing template, through the evaporation induced self-assembly (EISA) process. The issue of thermal and structural stability of a mesoporous TiO2 film was addressed via optimization of annealing temperature and time. An anatase phase, high crystallinity TiO2 film with ordered pores was obtained at 430 °C after annealing for 15 min. The synthesized film was crack free with TiO2 nanoparticle size of 10-15 nm, quasi-hexagonal pore diameter in the range of 8-10 nm and film thickness of ~ 150 nm. © 2009 Elsevier B.V. All rights reserved. | Source Title: | Materials Letters | URI: | http://scholarbank.nus.edu.sg/handle/10635/83136 | ISSN: | 0167577X | DOI: | 10.1016/j.matlet.2009.04.036 |
Appears in Collections: | Staff Publications |
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