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|Title:||Note: Application of a pixel-array area detector to simultaneous single crystal x-ray diffraction and x-ray absorption spectroscopy measurements|
|Citation:||Sun, C.-J., Zhang, B., Brewe, D.L., Chen, J.-S., Chow, G.M., Venkatesan, T., Heald, S.M. (2014). Note: Application of a pixel-array area detector to simultaneous single crystal x-ray diffraction and x-ray absorption spectroscopy measurements. Review of Scientific Instruments 85 (4) : -. ScholarBank@NUS Repository. https://doi.org/10.1063/1.4871055|
|Abstract:||X-ray diffraction (XRD) and X-ray absorption spectroscopy (XAS) are two main x-ray techniques in synchrotron radiation facilities. In this Note, we present an experimental setup capable of performing simultaneous XRD and XAS measurements by the application of a pixel-array area detector. For XRD, the momentum transfer in specular diffraction was measured by scanning the X-ray energy with fixed incoming and outgoing x-ray angles. By selecting a small fixed region of the detector to collect the XRD signal, the rest of the area was available for collecting the x-ray fluorescence for XAS measurements. The simultaneous measurement of XRD and X-ray absorption near edge structure for Pr0.67Sr0.33MnO3 film was demonstrated as a proof of principle for future time-resolved pump-probe measurements. A static sample makes it easy to maintain an accurate overlap of the X-ray spot and laser pump beam. © 2014 AIP Publishing LLC.|
|Source Title:||Review of Scientific Instruments|
|Appears in Collections:||Staff Publications|
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