Please use this identifier to cite or link to this item:
|Title:||Preliminary study of the analysis of oligogalacturonic acids by electrospray ionization mass spectrometry|
|Authors:||Zhu, L. |
|Citation:||Zhu, L., Lee, H.K. (2001). Preliminary study of the analysis of oligogalacturonic acids by electrospray ionization mass spectrometry. Rapid Communications in Mass Spectrometry 15 (12) : 975-978. ScholarBank@NUS Repository. https://doi.org/10.1002/rcm.326|
|Abstract:||During systematic studies of the behavior of oligogalacturonic acids (OGAs) under different conditions using electrospray ionization mass spectrometry (ESI-MS), cation adduction, fragmentation and non-covalent binding were found to be the three major problems that compromised the analysis of OGAs by ESI-MS. By adjusting solution components, capillary temperature and capillary voltage in the ESI source, an optimized condition was found that gave a clean and clear spectrum of trigalacturonic acid. A direct injection ESI-MS technique based on the use of aqueous acetonitrile and acetic acid and triethylamine (TEA) as modifiers has been applied to analyze a mixture including mono-, di- and trigalacturonic acids, which will facilitate further applications of ESI-MS in the analysis of mixtures of OGAs. © 2001 John Wiley & Sons, Ltd.|
|Source Title:||Rapid Communications in Mass Spectrometry|
|Appears in Collections:||Staff Publications|
Show full item record
Files in This Item:
There are no files associated with this item.
checked on Jul 17, 2018
WEB OF SCIENCETM
checked on Jun 27, 2018
checked on May 25, 2018
Items in DSpace are protected by copyright, with all rights reserved, unless otherwise indicated.